Report of the XIV SBPMat Meeting: plenary lectures with their files, memorial lecture, symposia, awards…

OPENING CEREMONY

Sunday, September 27. By 6:45 pm. Hundreds of people enter the plenary room of the Convention Center “SulAmérica”, in Rio de Janeiro (Brazil) for the opening ceremony of the 14th annual meeting of the Brazil Materials Research Society, whose acronym in Portuguese is SBPMat. The opening table is composed by the chairmen of the event, Prof. Marco Cremona (Brazil) and Prof. Fernando Lázaro Freire Junior (Brazil), as well as the present SBPMat president, Prof. Roberto Mendonça Faria (Brazil), the immediate past president of the European Materials Research Society (E-MRS), Prof. Rodrigo Martins (Portugal), and the general secretary of the International Union of Materials Research Societies (IUMRS), Prof. Robert Chang (USA). Behind them, a big banner shows the logos of dozens of institutions and companies that gave financial support to the event.

At the opening table, from the readers´ left: Prof. Rodrigo Martins (Portugal, E-MRS immediate past president and IUMRS officer), Prof. Fernando Lázaro Freire Junior (Brazil, chair of the event), Prof. Marco Cremona (Brazil, chair of the event), Prof. Roberto Mendonça Faria (Brazil, SBPMat president), and Prof. Robert Chang (USA, IUMRS general secretary).

Near 1,000 attendants are present at the ceremony, which starts with the Brazilian national anthem. The chair Prof. Cremona welcomes the participants to the meeting. Prof. Robert Chang, who was president of MRS (Materials Research Society) in 1989 and founded IUMRS in 1991, convokes the participants of all countries to try to solve together the most important global challenges for materials research, related to health, food, environment, transport etc. Representing E-MRS, Prof. Martins, who presently takes care of Global Leadership and Service Award at IUMRS, emphasizes his desire of promoting international connections. Prof. Faria talks a little bit about Brazil, which, as well as other developing countries, is very rich in raw materials but needs to add value to its products by means of science and technology.

After the opening, Prof. Eloisa Biasotto Mano (Brazil) goes to the stage for the Memorial Lecture “Joaquim da Costa Ribeiro“, which is a distinction bestowed annually by SBPMat on a Brazilian researcher with outstanding career in the field of Materials. This 91-year-old scientist pursued international scientific education at a time when most women were illiterate in Brazil, and founded in the Federal University of Rio de Janeiro (UFRJ) the first research group in polymers in the country. This group later became the Institute of Macromolecules (IMA), which was directed by Eloisa until she retired. In the memorial lecture, she talks about macromolecular materials and, using a representation of a polyethylene molecule made by herself with wire, she shows how these kind of molecules behave in response to their big size. A group of Prof. Eloisa´s disciples (among them, the present director of IMA) assists her with the presentation, showing affection, gratitude and admiration for her . After the talk, many attendants of diverse ages make a queue to take a picture with this protagonist of the dawn of polymer science in Brazil. Eloisa, who is professor emeritus of UFRJ, poses for all the pictures she is ask to. At the end of the photo session, she accepts our microphone and leaves a message for the young people starting a carreer in science:

Right after the memorial lecture, in the same venue, the participants enjoy the welcome cocktail while meeting friends and collaborators. The cocktail is animated by live “chorinho” music, an instrumental Brazilian popular genre original from Rio de Janeiro.

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PLENARY LECTURES

Nader Engheta

Nader Engheta.

Monday, September 28. At 8:30 in the morning, the plenary room is full of attendants waiting to learn about metamaterials and the extreme behavior of waves interacting with them in the first plenary lecture of the event. The speaker is Nader Engheta, the H. Nedwill Ramsey Professor of Electrical and Systems Engineering at the University of Pennsylvania (United States). This Iranian-born scientist is a recognized world leader in research on metamaterials, and holds an H number of 69. Through experimental and theoretical research, Engheta and his collaborators have created such unconventional things as nanocircuits made of metamaterials that function as optical filters. Since the beginning of the talk, Engheta captivates the audience with some history of science and with a world of structures created by using particular composite metamaterials with particular sizes and geometries and arranged in particular ways with the aim of obtaining unconventional interaction with light and other waves.

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Edgar Zanotto.

Edgar Zanotto.

In the afternoon, at 3:30, more than 400 people attend the second plenary lecture, which is about glass-ceramics (materials formed through controlled crystallization of certain glasses). The speaker is the Brazilian researcher Edgar Zanotto, Professor at the Federal University of São Carlos (UFSCar), in Brazil, where he founded and heads the Vitreous Materials Laboratory (LaMaV) that assembles a big international team. Zanotto, who is a world-renowned expert on glass-ceramics, presents in his lecture many useful applications of these materials, such as cooking hobs or artificial bones and teeth. He also mentions the scientists who, along 60 years of glass-ceramics history, contributed to the advancement of research on that topic. In spite of those contributions, the comprehension of some aspects of the formation of glass-ceramics is not complete, he says, but that is not a problem for glass-ceramics fabrication and applications. It´s just an opportunity for fundamental scientists.

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Paul Ducheyne. Biomaterials. Merging Materials Science with Biology.

Paul Ducheyne.

Tuesday, September 29. 8:30 am, time for the third plenary lecture of the event. The lecturer, Prof. Paul Ducheyne, also comes from University of Pennsylvania (USA), where he directs a multidisciplinary center for bioactive materials and tissue engineering research. An authority on biomaterials field, Ducheyne is the editor in chief of a six-volume book on biomaterials published in 2011. In the talk, he shows a series of biomaterial-made devices, grafts, scaffolds etc., most of them already being commercialized, that actively interact with the body, either by promoting tissue formation (for example, bone) or by releasing drugs for diverse treatments. Ducheyne presents their effects on solving health problems, numbers about their markets, and scientific recent advances that can make them even more effective.

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Ulrike Diebold. Surfaces of Metal Oxides.
Ulrike Diebold.

Some hours later, at 3:30 pm, hundreds of participants cluster again, this time around Prof. Ulrike Diebold, whose research group at UT Wien (Austria) is devoted to the understanding of fundamental mechanisms and processes occurring in surfaces at the atomic scale. Prof. Diebold catches the audience attention from the beginning to the end by showing, through scanning tunneling microscopy images, how she spies the behavior of atoms on the surface of metal oxides – topic in which she is a worldwide leader researcher. In particular, she reveals two secrets of metal oxide surfaces: the first one about how oxygen adsorbs on titanium dioxide and the second one about how active single metal atoms are in oxidation process in magnetite.

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George Malliaras.
George Malliaras.

Wednesday, September 30. In the plenary lecture of the morning, the audience is transported again to the social-impacting world of biomaterials by Prof. George Malliaras, Greek-born, working at École Nationale Supérieure des Mines de Saint-Étienne (France), where he heads the Department of Bioelectronics. Malliaras has an H index of 64. After many years working on organic electronics, he entered the new field of organic bioelectronics and obtained impacting results. His research is about electronic devices made of conducting polymers that match properties of living tissues. These devices are used for interfacing with human brain – a “natural electronic device”. The final purpose is to study brain activity or diagnose and even treat neurological diseases such as epilepsy. An example of device is a transistor that enables boosted in vivo recording of brain activity with low invasion. As suggestions for the materials community, Malliaras highlights the importance of collaboration with neuroscientists and physicians and the challenge of improving the understanding of electronic transport and structure.

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Ichiro Takeuchi. Combinatorial Approach to Materials Discovery.

Ichiro Takeuchi.

In the talk of the afternoon, the speed of science progress accelerates following the beat of the combinatorial approach. Prof. Ichiro Takeuchi, from University of Maryland (USA), explains how his group manages to optimize materials and properties discovery. As well as in lottery one can buy a big number of tickets to have more chances to win a prize, in materials discovery scientists can produce a huge number of combinations of elements to obtain a compound with desirable properties. For example, for quaternary compounds, millions of combinations are possible, from which only 0,01 % are known. In Prof. Takeuchi´s lab, machines for thin film deposition used with masks work night and day to create patchwork-like samples containing libraries of similar compounds. Then, the libraries are characterized by rapid tools, giving information about the properties of several compounds at the same time. Coupled with appropriate theory and computational simulations, these high-throughput experiments become real materials discovery engines.

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Claudia Draxl. On the Search of Novel Materials: Insight and Discovery though sharing of big data.
Claudia Draxl.

Thursday, October 1st, 8:30 am. In the last plenary lecture of the event, Prof. Claudia Draxl (Humboldt University, Germany) publicly wonders how to make available the huge amount of data resulting from experiments around the world, high-throughput screening, computer clusters etc. Why to do that with scientific data? For confirmation, broad dissemination in society, sharing with distant collaborators and reuse with new purposes. With that aim, Prof. Draxl and collaborators from European countries are facing the development of a repository of materials raw data, called Novel Materials Discovery (NoMaD), which hosts, organizes and shares materials data on the web.

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SYMPOSIA SESSIONS

Some of the symposia coordinators with the meeting chairs and the SBPMat president.

The symposia at SBPMat annual meetings are selected from proposals that can be submitted to the event committee by any scientist from anywhere in the world. This edition of the event encompassed 26 symposia (including the satellite event “8th International Summit on Organic and Hybrid Solar Cells Stability”) and 2 workshops, and it registered symposia coordinators from Argentina, Denmark, England, France, Germany, Italy, Ireland, Japan, Portugal, Spain, Swiss, USA, and, of course, Brazil. Within the symposia, near 190 invited speeches and more than 2,000 technical works are presented and discussed in oral and posters sessions, on a wide range of subjects going from carbon nanostructures to biomaterials, from characterization techniques to computer simulation, from materials for sustainable development to safe use of nanomaterials.

While some symposia have been held year after year in the SBPMat meeting, the University Chapters symposium was a novelty of this year meeting. It was completely organized by students from diverse points of Brazil who are coordinators of the SBPMat University Chapters. The chapters are organized teams, affiliated with the society, composed of graduate and undergraduate students working in materials field. The members of these groups carry out diverse activities that complement their academic education. The students from the existing chapters, which were eight in number up to the moment of the meeting, faced the challenge of organizing a symposium – a task that is usually done by senior researchers.

In fact, students have not only active but also massive participation in the XIV SBPMat meeting. Almost half of the attendants (950 people) were master, doctoral and even undergraduate students doing research on materials field. In Brazil, the federal agency for research support, CNPq, has a program called “scientific initiation” that grants scholarships to undergraduate students to conduct research under the supervision of a Professor.

For the oral sessions of the symposia, all along the meeting, after the morning plenary session, and before and after the afternoon plenary talks, the attendants distributed themselves among 17 rooms. The poster sessions took place at the end of the afternoon from Monday to Wednesday and in the morning on Thursday. Walking through the long corridors of the poster sessions, one could see active scientific discussion, many times between a young author and a renowned researcher. One could also hear very positive comments about the original arrangement of the poster panels. The size of the poster session was impressive. In total, near 1,800 research works were presented in the posters.

View of the first poster session.

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EXHIBITION

Twice a day from Monday to Wednesday, the attendants could take a break and have a coffee with cookies while visiting the exhibition of the event, which encompassed 32 stands showing a variety of scientific instruments, services, scientific journals, books and opportunities for the materials community. In addition, on Wednesday, the participants had the opportunity to attend four hours of technical talks given by some expositors about fabrication and characterization techniques.

Coffee break and exhibition.

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CLOSING AND AWARDS CEREMONY

On Thursday by 12:30 the closing ceremony started. In the closing panel, Prof. Soo Wohn Lee, from MRS Korea and conference chair of the IUMRS-ICAM 2015, joined the representatives of SBPMat, E-MRS and IUMRS.

In his final remarks, the meeting chair Prof. Cremona presented some photos of the past days and hours that made the public remember so nice and fruitful moments. He also presented the numbers of the event: 2,000 registered people from 985 institutions, among which 300 were foreign researchers from 40 countries. Finally, he announced that the next SBPMat annual meeting will be held in Campinas city (São Paulo state).

After the closing words, more than 20 prizes were given to young researchers within four different awards: the Bernhard Gross Award, a traditional SBPMat recognition for the best works of students, and the awards bestowed by IUMRS, E-MRS and Horiba.

Announcement of the students who won the Bernhard Gross Award.

See list of the awards winners.

Interviews with plenary speakers of the XIV SBPMat Meeting: Ichiro Takeuchi.

The search for the materials that are most suitable for performing certain tasks maybe exists since the dawn of humanity. In this search, on the opposite end to the trial and error method, there is the combinatorial approach, which aims to increase the efficiency of the process of discovering or producing materials. This approach is based on the screening of large amounts of materials with compositions slightly different one another, using databases, rapid synthesis and characterization techniques, simulations, robots and other tools. The combinatorial approach has been applied to the pharmaceutical industry since the 1990s to identify new and useful compounds, and it also has its place in the field of Materials Science and Engineering.

Prof. Ichiro Takeuchi

During the XIV SBPMat Meeting, Professor Ichiro Takeuchi will give a plenary talk on the combinatorial approach to materials discovery – an issue that is part of his daily life. Takeuchi is a Professor of the Materials Science and Engineering Department at the University of Maryland, in the United States, since 1999. In this institution, he leads the Combinatorial Synthesis and Rapid Characterization Center and the Keck Lab for Combinatorial Nanosynthesis/ Multiscale Characterization. He is a Visiting Professor at the Tokyo University of Science since 2010. He is also member of the Executive Committee of the Forum on Industrial & Applied Physics from the American Physical Society (APS). 

Takeuchi graduated with a Degree in Physics in 1987 at the California Institute of Technology (Caltech). For four years he worked in Japan at the microelectronics research laboratories of the NEC Corporation, to later return to the United States. In 1996, he earned his Ph.D. at the University of Maryland. Then, he went to the Lawrence Berkeley National Laboratory, where he stayed until 1999 as a postdoctoral researcher. In 2004, he was the chairman of the Gordon Conference on Combinatorial and High-throughput Materials Science. In 2009, he founded a company dedicated to the development of materials and systems for applications in the field of energy, the Maryland Energy and Sensor Technologies, LLC.

Ichiro Takeuchi was a Visiting Professor at universities in Japan and Germany. He has received awards and distinctions from the National Science Foundation (Career Award), the Office of Naval Research in the US (Young Investigator Program Award) and the University of Maryland, among other institutions. The scientist, whose H index is 40, according to Google Scholar, is the author of over 180 papers, with more than 5,900 citations, and a book on the combinatorial synthesis of materials.

What follows is a brief interview with this plenary speaker.

SBPMat newsletter: – Help us to visualize how the combinatorial research is performed. For instance, choose an example of a material created in your laboratories with this approach, and outline the “step-by-step”.

Synthesis of thin-film combinatorial library: in this example, co-sputtering (a) is used to generate large compositional variation across a 3” wafer (b); such a sample is called a composition spread wafer; the composition variation is mapped on to ternary compositional phase diagram using electron probe (c).

Ichiro Takeuchi: – We do thin film based combinatorial materials research. The goal is to carry out rapid screening of previously unexplored compositional landscape in order to discover new materials with enhanced physical properties. We make wafers or chips where there are large composition variations in deposited thin films. Sometimes the thin films are separated into different pads, and sometimes it is one continuous film with changing composition across the wafer. We want the variation to be as large and diverse as possible, so that we can map large compositional variation in a single experiment. We then take different characterization techniques to carry out rapid screening of various physical properties. For example, right now, we have a project to search for new permanent magnet materials. For this, we use techniques such as scanning SQUID or scanning magneto-optical Kerr effect measurements. These measurements can be used to map magnetic properties of all the compositions on a single wafer. These wafers and chips are called combinatorial libraries. We also do a lot of structural characterization. For this purpose, we often go to synchrotron beamlines. At such locations, because of the large beam flux, we are able to carry out x-ray diffraction of the entire wafer very quickly. Right now, we can scan 200-300 spots in 2 hours.

SBPMat newsletter: – In your opinion, what are your most significant contributions in the field of combinatorial materials science? Please explain them, very briefly, and share references from the resulting articles or books, or comment if these studies have produced patents, products, spin-off companies etc.

Examples of combinatorial libraries of functional materials and visualization of their data: (a) permanent magnet library for systematic investigation of exchange coupling showing magnetic hysteresis loops taken at each spot on the library (from Physical Review B75, 144429 (2007)); (b) ferroelectric library displaying ferroelectric hysteresis loops measured at each spot (from Journal of Materials Research 27, 2691 (2012)); (c) superconductor library with resistance – temperature curves mapped onto the positions where they were measured (from APL Materials 1, 042101 (2013)).

Ichiro Takeuchi: – Over the years, we have carried out combinatorial investigation on a variety of topics in the general field of functional materials. They include superconductors, shape memory alloys, magnetosrictive materials, ferroelectric and dielectric materials to name a few. In carrying out such experiments, we have had to develop and establish techniques to effectively implement the strategies. We have indeed discovered a number of new compounds. For instance, working together with theoretical colleagues, we have found shape memory alloys with long fatigue lives. I have patents on a number of low-loss dielectric materials as well as novel piezoelectric materials. Many groups are now doing follow-on work on a lead-free morphotropic phase boundary piezoelectric material we found a number of years ago. In addition to the materials that were discovered, we have established combinatorial strategies as a technique to rapidly delineate composition-structure-property relationships in different materials systems. We have recently published a comprehensive review article. It is: “Applications of high throughput (combinatorial) methodologies to electronic, magnetic, optical, and energy-related materials,” Journal of Applied Physiscs 113, 231101 (2013) by Martin L. Green, Ichiro Takeuchi, and Jason R. Hattrick-Simpers.

SBPMat newsletter: -If you wish, leave a message or an invitation to your plenary talk to the readers who will attend the XIV SBPMat Meeting.

Ichiro Takeuchi: – The notion of search and discover is central to materials research. The combinatorial methodology is the natural counterpart to the concerted efforts in theoretical design of materials taking place around the world. By effectively coupling theory with high-throughput experimentation, we can really accelerate the rate at which new materials are discovered. I will present a mode of research we call “integrated materials engine” where theory and experiments are woven together and built on a flexible database and data management platform.

Integrated materials discovery engine: we propose coupling of high-throughput combinatorial materials exploration with theoretical investigation. Multiple feedback points between the two tracks ensure that we carry out accelerated exploration effectively.

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